1-Propylboronic acid → HCID 67397137, 화합물

HRID 869729

반응식

HRID 869729 반응식
Cl[C:2]1[N:7]=[C:6]([C:8]([O:10][CH2:11][CH3:12])=[O:9])[C:5]([CH3:13])=[N:4][CH:3]=1.[CH2:14](B(O)O)[CH2:15][CH3:16]>>[CH3:13][C:5]1[C:6]([C:8]([O:10][CH2:11][CH3:12])=[O:9])=[N:7][C:2]([CH2:14][CH2:15][CH3:16])=[CH:3][N:4]=1

참가 물질

3

반응물 2

HCID 3510651-Propylboronic acidHCID 87384166HCID 87384166, 화합물

생성물 1

HCID 67397137HCID 67397137, 화합물

실험 절차

The preparation was performed in a similar manner as Reference Example 1.13 (d) from ethyl 6-chloro-3-methylpyrazine-2-carboxylate (Reference Example 1.13 (c)) (1.50 g, 7.48 mmol) and n-propylboronic acid (1.32 g, 15.0 mmol) to give ethyl 3-methyl-6-propylpyrazine-2-carboxylate. MS (APCI): m/z 209 (M+H).

출처 및 근거

ORD 기록
ord-b64fd4d29759401892e2e8e56af408a3
출처 데이터셋
uspto-grants-2015_03
특허 번호
US08969376B2

연결된 노트

불러오는 중…