Gallium(III) nitrate hydrate → Gallium nitrate

HRID 871824

반응식

HRID 871824 반응식
O.[N+:2]([O-:5])([O-:4])=[O:3].[Ga+3:6].[N+:7]([O-:10])([O-:9])=[O:8].[N+:11]([O-:14])([O-:13])=[O:12]>O>[N+:2]([O-:5])([O-:4])=[O:3].[Ga+3:6].[N+:7]([O-:10])([O-:9])=[O:8].[N+:11]([O-:14])([O-:13])=[O:12]

참가 물질

3

반응물 1

HCID 11550823Gallium(III) nitrate hydrate

생성물 1

HCID 61635Gallium nitrate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

The stoichiometric amount of gallium-(III)-nitrate hydrate (5.031 g) was dissolved in 80 mL of deionised water to yield gallium nitrate solution. On the other hand, 1.27 g of ammonium metavanadate were dissolved in 100 mL of deionised water at 80° C. The two solutions obtained were mixed under continuous stirring and the pH of the mixture obtained was adjusted to 7 by adding 24% aqueous ammonia solution. A precipitate formed and the suspension obtained was stirred for another half an hour and filtered. The solid obtained was washed several times with deionised water and dried at 120° C. overnight. 2 g of gallium vanadate were obtained and analytically characterised.

출처 및 근거

ORD 기록
ord-1597308fbc9f44ae94f281a4b8999a95
출처 데이터셋
uspto-grants-2015_03
특허 번호
US08975206B2

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