Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene → Methyl 2-nitrobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene | HCID 241 | — |
| 반응물 | 2-Nitrobenzoic acid | HCID 11087 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | Methyl 2-nitrobenzoate | HCID 69072 | — |
반응 단계
A solution of 6-nitro-benzoic acid in benzene was treated with thionyl chloride (2.5 eq) and stirred at reflux for 8 h. After evaporation, the residue was dissolved in chloroform and then treated with methanol. After stirring at reflux for 3 h, the mixture was evaporated to afford compound 3.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08980901B2 |
| 출처 데이터셋 | uspto-grants-2015_03 |
| ORD ID | ord-3ab26dc5f94c470a80020d25845e6083 |
| 출처 메모 | uspto-grants-2015_03 |