Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3-Dinitrophenol → Sodium dinitrophenolate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3-Dinitrophenol | HCID 6191 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Sodium dinitrophenolate | HCID 86649331 | — |
반응 단계
The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH (1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08987411B2 |
| 출처 데이터셋 | uspto-grants-2015_03 |
| ORD ID | ord-bb64b922e5af466a87709b09e9ad12cb |
| 출처 메모 | uspto-grants-2015_03 |