N'-(3-(Dimethylamino)propyl)-N,N-dimethyl-1,3-propanediamine → (E)-N,N-bis(3-(dimethylamino)propyl) dec-2-enamide

반응식

[C:1]([OH:12])(=O)/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH3:13][N:14]([CH3:25])[CH2:15][CH2:16][CH2:17][NH:18][CH2:19][CH2:20][CH2:21][N:22]([CH3:24])[CH3:23]>>[CH3:24][N:22]([CH3:23])[CH2:21][CH2:20][CH2:19][N:18]([CH2:17][CH2:16][CH2:15][N:14]([CH3:13])[CH3:25])[C:1](=[O:12])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

참가 물질

반응물 2

HCID 81207N'-(3-(Dimethylamino)propyl)-N,N-dimethyl-1,3-propanediamine

HCID 5282724trans-2-Decenoic acid

생성물 1

HCID 86694814(E)-N,N-bis(3-(dimethylamino)propyl) dec-2-enamide

실험 절차

The same operation as in Example 1-1 or 1-2 was carried out using trans-2-decenoic acid and N-(3-(dimethylamino)propyl)-N′,N′-dimethylpropane-1,3-diamine as starting materials to give the aimed compound.

출처 및 근거

ORD 기록: ord-d4640b67cd524f97982bcdc417ebda22
출처 데이터셋: uspto-grants-2015_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08987486B2

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