Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → Benzyl 4-chlorobenzoyloxycarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| 반응물 | Benzyl hydroxycarbamate | HCID 18907 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Benzyl 4-chlorobenzoyloxycarbamate | HCID 51033117 | — |
반응 단계
4-Chlorobenzoyl chloride (13.1 mL, 102 mmol) is added slowly to a solution of benzyl hydroxycarbamate (19.0 g, 114 mmol) and triethylamine (14.4 mL, 104 mmol) in diethyl ether (500 mL) at 0° C. then stirred at room temperature for 1 h. The reaction is
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08987504B2 |
| 출처 데이터셋 | uspto-grants-2015_03 |
| ORD ID | ord-61ae2cfa3efb4b06b28f8c9207977e98 |
| 출처 메모 | uspto-grants-2015_03 |