4-Chlorobenzoyl chloride → tert-Butyl (4-Chlorobenzoyl)oxycarbamate

HRID 879024노트

반응식

HRID 879024 반응식
[OH:1][NH:2][C:3](=[O:9])[O:4][C:5]([CH3:8])([CH3:7])[CH3:6].[Cl:10][C:11]1[CH:19]=[CH:18][C:14]([C:15](Cl)=[O:16])=[CH:13][CH:12]=1>C(Cl)Cl>[Cl:10][C:11]1[CH:19]=[CH:18][C:14]([C:15]([O:1][NH:2][C:3](=[O:9])[O:4][C:5]([CH3:8])([CH3:7])[CH3:6])=[O:16])=[CH:13][CH:12]=1

참가 물질

4

반응물 2

HCID 85014-Chlorobenzoyl chlorideHCID 97534tert-butyl N-hydroxycarbamate

생성물 1

HCID 23655003tert-Butyl (4-Chlorobenzoyl)oxycarbamate

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

To a solution of tert-butyl hydroxycarbamate (9.76 g, 73.3 mmol) in DCM (120 mL) at 0° C., is added 4-chlorobenzoyl chloride (8.13 mL, 73.3 mmol) followed by the dropwise addition of

후처리

  1. additionfollowed by the dropwise addition of

출처 및 근거

ORD 기록
ord-7c4cff7d7ff94ee292992348b3cbb040
출처 데이터셋
uspto-grants-2015_03
특허 번호
US08987504B2

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