Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → 8-Dodecen-1-ol, 1-acetate, (8Z)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 8-Dodecen-1-ol, (8Z)- | HCID 5283295 | — |
| 반응물 | 11-Hexadecenal, (11Z)- | HCID 5364495 | — |
| 생성물 | 8-Dodecen-1-ol, 1-acetate, (8Z)- | HCID 5363377 | 90% |
반응 단계
By acetylation of compound 2: According to the procedure for compound 6, Ac2O (0.29 mL, 3.0 mmol), pyridine (0.14 mL, 1.8 mmol), and alcohol 12 (0.28 g, 1.5 mmol) were reacted to provide 13 (19 g, 90% yield, 86% Z as determined by 1H-NMR) as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08987531B2 |
| 출처 데이터셋 | uspto-grants-2015_03 |
| ORD ID | ord-8d0a89f683b240769b5490826310d381 |
| 출처 메모 | uspto-grants-2015_03 |