Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-Fluoro-4-nitrobenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Fluoro-4-nitrobenzoic acid | HCID 230653 | — |
| 생성물 | 3-Fluoro-4-nitrobenzoyl chloride | HCID 2774656 | 99% |
반응 단계
A stirred solution of 3-fluoro-4-nitro-benzoic acid (1.65 g, 8.91 mmol) in thionyl chloride (10 mL) was heated at reflux for 2 h. Excess thionyl chloride was evaporated in vacuo and the residue azeotroped with toluene to afford 3-fluoro-4-nitro-benzoyl chloride (1.7 g, 99%) as a brown oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08993574B2 |
| 출처 데이터셋 | uspto-grants-2015_03 |
| ORD ID | ord-8da9e7ed9518459a824ff103d4a188b8 |
| 출처 메모 | uspto-grants-2015_03 |