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Lithium hexamethyldisilazane → 1-tert-butyl 4-ethyl 4-((5-bromo-1-tert-butyl-1H-pyrazol-4-yl)methyl)piperidine-1,4-dicarboxylate

HRID 880884
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HRID 880884 반응식
[N:1]1([C:12]([O:14][C:15]([CH3:18])([CH3:17])[CH3:16])=[O:13])[CH2:6][CH2:5][CH:4]([C:7]([O:9][CH2:10][CH3:11])=[O:8])[CH2:3][CH2:2]1.C[Si]([N-][Si](C)(C)C)(C)C.[Li+].[Br:29][C:30]1[N:34]([C:35]([CH3:38])([CH3:37])[CH3:36])[N:33]=[CH:32][C:31]=1[CH2:39]Br>C1COCC1>[Br:29][C:30]1[N:34]([C:35]([CH3:37])([CH3:36])[CH3:38])[N:33]=[CH:32][C:31]=1[CH2:39][C:4]1([C:7]([O:9][CH2:10][CH3:11])=[O:8])[CH2:3][CH2:2][N:1]([C:12]([O:14][C:15]([CH3:17])([CH3:16])[CH3:18])=[O:13])[CH2:6][CH2:5]1
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HCID 2733832Lithium hexamethyldisilazaneHCID 27588121-Tert-butyl 4-ethyl piperidine-1,4-dicarboxylateHCID 674914615-Bromo-4-(bromomethyl)-1-(tert-butyl)-1H-pyrazole

생성물 1

HCID 674915481-tert-butyl 4-ethyl 4-((5-bromo-1-tert-butyl-1H-pyrazol-4-yl)methyl)piperidine-1,4-dicarboxylate수율 48%

시약·촉매·용매 1

HCID 8028
Tetrahydrofuran
용매
2회

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온도
-78 °C

실험 절차

A solution of 1-tert-butyl 4-ethyl piperidine-1,4-dicarboxylate (0.37 mL, 1.47 mmol) in THF (15 mL) was cooled to −78° C. and then treated with lithium bis(trimethylsilyl) amide (1.48 mL, 1.48 mmol, 1 M toluene), dropwise. The reaction was stirred 15 minutes at −78° C., warmed to 0° C. for 30 minutes and then cooled back to −78° C. A solution of 5-bromo-4-(bromomethyl)-1-tert-butyl-1H-pyrazole (335 mg, 1.13 mmol) in THF (10 mL) was added, the mixture was stirred 1 hour at −78° C., and then allowed to stir 18 hours at room temperature. The reaction was quenched with saturated aqueous ammonium chloride (20 mL), stirred 30 minutes at room temperature, diluted with water (50 mL) and extracted with ethyl acetate (2×50 mL). The organics were combined, dried over sodium sulfate, filtered and concentrated. The resultant residue was purified by flash chromatography (5-40% ethyl acetate/heptane, 25 g silica gel) to yield 256 mg of 1-tert-butyl 4-ethyl 4-((5-bromo-1-tert-butyl-1H-pyrazol-4-yl)methyl)piperidine-1,4-dicarboxylate as a clear oil. +ESI (M+H) 474.2, (M+2+H) 476.2; 1H NMR (400 MHz, CDCl3, δ): 7.20 (s, 1H), 4.16 (q, J=7.2 Hz, 2H), 3.93 (br. s., 2H), 2.84 (m, 2H), 2.66 (s, 2H), 2.10 (d, J=12.5 Hz, 2H), 1.72 (s, 9H), 1.45 (m, 11H), 1.25 (t, J=7.1 Hz, 3H).

후처리

  1. temperaturewarmed to 0° C. for 30 minutes
  2. temperaturecooled back to −78° C
  3. stirringthe mixture was stirred 1 hour at −78° C.
  4. stirringto stir 18 hours at room temperature
  5. customThe reaction was quenched with saturated aqueous ammonium chloride (20 mL)
  6. stirringstirred 30 minutes at room temperature
  7. additiondiluted with water (50 mL)
  8. extractionextracted with ethyl acetate (2×50 mL)
  9. dry with materialdried over sodium sulfate
  10. filtrationfiltered
  11. concentrationconcentrated
  12. customThe resultant residue was purified by flash chromatography (5-40% ethyl acetate/heptane, 25 g silica gel)

출처 및 근거

ORD 기록
ord-21df24c3b668486cbc598820a4b66385
출처 데이터셋
uspto-grants-2015_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08993586B2

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