Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,7-Diphenyl-4-heptanol → HCID 178418375, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,7-Diphenyl-4-heptanol | HCID 10539870 | — |
| 반응물 | HCID 178418459 | HCID 178418459 | — |
| 반응물 | HCID 178418471 | HCID 178418471 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 178418375 | HCID 178418375 | — |
반응 단계
The alcohol 137 was prepared from the crude aldehyde 136. and 1.5 mL (0.75 mmol) of 120 in 2.0 mL of THF as described above for the synthesis of alcohol 121 in Example 1 to give 220 mg of the crude diastereomeric alcohol 137. Flash chromatography (elution with 20% ethyl acetate in hexane) afforded 146 mg of the alcohol 137 as an oil. 1H NMR consistent with structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723459 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-a6be5895ebf2488a874923e3878acfbe |
| 출처 메모 | uspto-grants-1998_03 |