2-Methylbenzoyl chloride → 2-Cyclohexyl-4,4-dimethyl-1-[(2-methylphenyl)carbonyl]-1,2-diazetidin-3-one

HRID 888859노트

반응식

HRID 888859 반응식
[CH:1]1([N:7]2[C:10](=[O:11])[C:9]([CH3:13])([CH3:12])[NH:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:14][C:15]1[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=1[C:17](Cl)=[O:18]>>[CH:1]1([N:7]2[C:10](=[O:11])[C:9]([CH3:13])([CH3:12])[N:8]2[C:17]([C:16]2[CH:20]=[CH:21][CH:22]=[CH:23][C:15]=2[CH3:14])=[O:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

참가 물질

3

반응물 2

HCID 702762-Methylbenzoyl chlorideHCID 673030222-Cyclohexyl-4,4-dimethyl-1,2-diazetidin-3-one

생성물 1

HCID 593615082-Cyclohexyl-4,4-dimethyl-1-[(2-methylphenyl)carbonyl]-1,2-diazetidin-3-one

실험 절차

2-Cyclohexyl-4,4-dimethyl-1,2-diazetidin-3-one prepared in Process 5 of Example 68 and 2-methylbenzoyl chloride were used for a similar reaction and treatment as Example 96, and the title compound was obtained as a colorless oil.

후처리

  1. customwere used for a similar reaction and treatment as Example 96

출처 및 근거

ORD 기록
ord-dfdb1b8641544e5f9ce0663fddba944e
출처 데이터셋
uspto-grants-2012_08
특허 번호
US08252781B2

반응 노트

불러오는 중…