Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazinecarboxylic acid, ethyl ester → HCID 178473566, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazinecarboxylic acid, ethyl ester | HCID 20064 | — |
| 반응물 | 4,5-Dihydro-2-(methylthio)thiazole | HCID 88324 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178473566 | HCID 178473566 | 25.5% |
반응 단계
A mixture of ethyl carbazate (23.4 g), 2-(methylthio)-2-thiazoline (25 g) and ethanol (250 ml) was heated to reflux for 3 days. It was then stirred at room temperature for 2 days. The precipitate was collected by filtration and washed with ethanol to obtain the title compound (9.05 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08252810B2 |
| 출처 데이터셋 | uspto-grants-2012_08 |
| ORD ID | ord-9e029b7850754c5e9764887691467095 |
| 출처 메모 | uspto-grants-2012_08 |