Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → Acenaphtho[1,2-b]quinoxaline-9-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | Acenaphthenequinone | HCID 6724 | — |
| 반응물 | 3,4-Diaminobenzoic acid | HCID 69263 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Acenaphtho[1,2-b]quinoxaline-9-carboxylic acid | HCID 626833 | — |
반응 단계
500 mL of dimethylformaldehyde was added to a mixture of 10 g of purified acenaphthenequinone and 84 g of 3,4-diaminobenzoic acid. The reactant continued to be stirred at room temperature for 21 hours. The precipitate was filtered to obtain a crude composition. This crude composition was dissolved in heated dimethylformamide, filtered again and purified by washing in dimethylformamide and water.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08253899B2 |
| 출처 데이터셋 | uspto-grants-2012_08 |
| ORD ID | ord-b46fb59434f14a34b3ceac798cedf565 |
| 출처 메모 | uspto-grants-2012_08 |