3-Butylpentane-2,4-dione → 2-[4-(4-Butyl-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol

HRID 891066노트

반응식

HRID 891066 반응식
Cl.[NH:2]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][OH:12])=[CH:6][CH:5]=1)[NH2:3].[CH2:13]([CH:17]([C:21](=O)[CH3:22])[C:18](=O)[CH3:19])[CH2:14][CH2:15][CH3:16]>>[CH2:13]([C:17]1[C:18]([CH3:19])=[N:3][N:2]([C:4]2[CH:5]=[CH:6][C:7]([CH2:10][CH2:11][OH:12])=[CH:8][CH:9]=2)[C:21]=1[CH3:22])[CH2:14][CH2:15][CH3:16]

참가 물질

3

반응물 2

HCID 737633-Butylpentane-2,4-dioneHCID 222447112-(4-Hydrazinophenyl)ethanol hydrochloride

생성물 1

HCID 222446452-[4-(4-Butyl-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol

실험 절차

The title compound was prepared according to the procedure described in step 1 of Example 1 from 2-(4-hydrazinophenyl)ethanol hydrochloride and 3-n-butyl-2,4-pentanedione: MS (ESI) m/z 273 [M+H]+, 1H-NMR (CDCl3) δ 7.37-7.26 (4H, m), 3.87 (2H, t, J=6.8 Hz), 2.91 (2H, t, J=6.6 Hz), 2.39 (2H, t, J=7.6 Hz), 2.25 (3H, s), 2.22 (3H, s), 1.53-1.26 (4H, m), 0.94 (3H, t, J=7.1 Hz).

출처 및 근거

ORD 기록
ord-032491315a414c72abced4deddc4955c
출처 데이터셋
uspto-grants-2006_02
특허 번호
US07001917B2

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