Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Trifluoromethyl)benzenesulfonamide → N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-4-(trifluoromethyl)benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Trifluoromethyl)benzenesulfonamide | HCID 70018 | — |
| 반응물 | Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate | HCID 22244550 | — |
| 생성물 | N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-4-(trifluoromethyl)benzenesulfonamide | HCID 22244534 | — |
반응 단계
The title compound was prepared according to the procedure described in step 2 of Example 22 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 4-(trifluoromethyl)benzenesulfonamide: 1H-NMR (CDCl3) δ 8.06 (2H, d, J=7.7 Hz), 7.80 (2H, d, J=8.2 Hz), 7.47-7.21 (9H, m), 6.10 (1H, br.s), 3.50-3.43 (2H, m), 2.86 (2H, t, J=6.3 Hz), 2.32 (3H, s), 2.23 (3H, s).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07001917B2 |
| 출처 데이터셋 | uspto-grants-2006_02 |
| ORD ID | ord-2a94aba85be3483385a5919f87aa30a7 |
| 출처 메모 | uspto-grants-2006_02 |