3,4-Difluorobenzenesulfonamide → HCID 10239282, 화합물
반응식
[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23](=O)[O:24]C3C=CC=CC=3)=[CH:16][CH:15]=2)[N:3]=1.[F:32][C:33]1[CH:34]=[C:35]([S:40]([NH2:43])(=[O:42])=[O:41])[CH:36]=[CH:37][C:38]=1[F:39]>>[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23]([NH:43][S:40]([C:35]3[CH:36]=[CH:37][C:38]([F:39])=[C:33]([F:32])[CH:34]=3)(=[O:41])=[O:42])=[O:24])=[CH:16][CH:15]=2)[N:3]=1참가 물질
3
실험 절차
The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 3,4-difluorobenzenesulfonamide: 1H-NMR (CDCl3) δ 7.84-7.70 (2H, m), 7.47-7.21 (10H, m), 6.07 (1H, br.s), 3.50-3.43 (2H, m), 2.85 (2H, t, J=6.3 Hz), 2.32 (3H, s), 2.22 (3H, s).
출처 및 근거
- ORD 기록
- ord-7d460a0169344e39b45dfab6e3ca3fdc
- 출처 데이터셋
- uspto-grants-2006_02