2-Fluorobenzenesulfonamide → 2-Fluoro-N-{[(2-{4-[5-methyl-4-phenyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}ethyl)amino]carbonyl}benzenesulfonamide

참여 물질

반응 단계

The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-{4-[5-methyl-4-phenyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}ethylcarbamate (step 7 of Example 52) and 2-fluoro-benzenesulfonamide: MS (ESI) m/z 547 [M+H]+, 545 [M−H]−, 1H-NMR (CDCl3) δ 7.86-7.81 (1H, m), 7.74-7.58 (1H, m), 7.48-7.24 (1H, m), 6.45 (1H, br.s) 3.54-3.49 (2H, m), 2.87 (2H, t, J=6.7 Hz), 2.23 (3H, s).

출처 및 근거