Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isobutylene → N-(4-ethylphenyl)maleimide isobutene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isobutylene | HCID 8255 | — |
| 반응물 | N-(4-Ethylphenyl)maleimide | HCID 522624 | — |
| 반응물 | Neodecanoate | HCID 21225528 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-(4-ethylphenyl)maleimide isobutene | HCID 69501763 | — |
반응 단계
In a one-liter autoclave were charged 400 ml of toluene as a polymerization solvent, 0.001 moles of perbutyl neodecanoate as a polymerization initiator, 0.42 moles of N-(4-ethylphenyl)maleimide, and 4.05 moles of isobutene, and the mixture was subjected to polymerization reaction under a polymerization condition at a polymerization temperature of 60° C. for a polymerization time of 5 hours, to obtain N-(4-ethylphenyl)maleimide-isobutene alternating copolymer. The thus obtained N-(4-ethylphenyl)maleimide-isobutene alternating copolymer had a weight average molecular weight (Mw) (as reduced into standard polystyrene) of 155,000 and an Mw/Mn of 2.6.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07001967B2 |
| 출처 데이터셋 | uspto-grants-2006_02 |
| ORD ID | ord-5c0a5748989048e88fb11a8d59533928 |
| 출처 메모 | uspto-grants-2006_02 |