2-Furancarbonyl chloride → N-[2-(3,4-methylenedioxyphenyl)ethyl]furan-2-carboxamide

HRID 892451

반응식

HRID 892451 반응식
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6](Cl)=[O:7].[CH2:9]1[O:20][C:19]2[CH:18]=[CH:17][C:13]([CH2:14][CH2:15][NH2:16])=[CH:12][C:11]=2[O:10]1>ClCCl.C(N(CC)CC)C>[CH2:9]1[O:20][C:19]2[CH:18]=[CH:17][C:13]([CH2:14][CH2:15][NH:16][C:6]([C:2]3[O:1][CH:5]=[CH:4][CH:3]=3)=[O:7])=[CH:12][C:11]=2[O:10]1

참가 물질

5

반응물 2

HCID 682422-Furancarbonyl chlorideHCID 738741,3-Benzodioxole-5-ethanamine

생성물 1

HCID 861822N-[2-(3,4-methylenedioxyphenyl)ethyl]furan-2-carboxamide

시약·촉매·용매 2

HCID 8471Triethylamine촉매HCID 6344Dichloromethane용매

실험 절차

N-[2-(3,4-methylenedioxyphenyl)-ethyl]furan-2-carboxamide was prepared by condensation of 2-furoyl chloride and 3,4-methylenedioxyphenethylamine in dichloromethane with triethylamine as catalyst.

출처 및 근거

ORD 기록
ord-b5738b13041c41049dcb5086eab2ca08
출처 데이터셋
uspto-grants-1992_06
특허 번호
US05118690

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