Ammonium Hydroxide → 5-(4-Chlorophenyl)furan-2-carboxamide

HRID 892687

반응식

HRID 892687 반응식
[NH4+:1].[OH-].[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[O:14][C:13]([C:15](Cl)=[O:16])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1>>[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[O:14][C:13]([C:15]([NH2:1])=[O:16])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1

참가 물질

3

반응물 2

HCID 14923Ammonium HydroxideHCID 27719705-(4-chlorophenyl)furan-2-carbonyl Chloride

생성물 1

HCID 47800015-(4-Chlorophenyl)furan-2-carboxamide

실험 절차

To 1000 ml. of cold, stirring NH4OH, 63 g. (0.26 mole) of 5-(p-chlorophenyl)-2-furoyl chloride is added portionwise. The resulting mixture is stirred at ice bath temperature for 15 minutes and then is stored at room temperature for 18 hours. The solid is filtered, is washed with water and is dried at 60 to yield 56 g. (97%).

후처리

  1. waitis stored at room temperature for 18 hours
  2. filtrationThe solid is filtered
  3. washis washed with water
  4. customis dried at 60
  5. customto yield 56 g

출처 및 근거

ORD 기록
ord-a4006aa4880e431ea97cf944de3c6cef
출처 데이터셋
uspto-grants-1992_06
특허 번호
US05118708

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