Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 4-(2-Methoxyethyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 4-Hydroxyphenylglyoxal dimethyl acetal | HCID 19788847 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 4-(2-Methoxyethyl)phenol | HCID 92516 | 59% |
반응 단계
The procedure of Example 2 was repeated with a solution of 3.00 g (15.3 mmol) 4-hydroxyphenylglyoxal dimethyl acetal in 10 g methanol containing 0.16 g (4.4 mmol) hydrogen chloride and 0.15 g moist 10% Pd/C catalyst being reacted with hydrogen gas pressurized at 300 psig at 50° C. 300 rpm. A 59% yield of 4-(2'-methoxyethyl)phenol was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05124489 |
| 출처 데이터셋 | uspto-grants-1992_06 |
| ORD ID | ord-c8d27b60dd4f4624ba1f8e4193a867b2 |
| 출처 메모 | uspto-grants-1992_06 |