Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 4-(2-Methoxyethyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 4-Hydroxyphenylglyoxal dimethyl acetal | HCID 19788847 | — |
| 생성물 | 4-(2-Methoxyethyl)phenol | HCID 92516 | 47% |
반응 단계
The procedure of Example 2 was repeated with a solution of 2.00 g (10.2) mmol) 4-hydroxyphenylglyoxal dimethyl acetal in 10 g methanol containing 0.37 g (10.2 mmol) hydrogen chloride and a 0.20 g dry 10% Pd/C catalyst being reacted with hydrogen gas pressurized at 50 psig at 25° C. A 47% yield of 4-(2'-methoxyethyl)phenol was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05124489 |
| 출처 데이터셋 | uspto-grants-1992_06 |
| ORD ID | ord-d12f1b3bc7654c74aa26163577d4b7bc |
| 출처 메모 | uspto-grants-1992_06 |