HCID 22399584, 화합물 → HCID 21479718, 화합물

HRID 893483노트

반응식

HRID 893483 반응식
[NH2:1][C:2]([C:4]1[CH:33]=[CH:32][C:7]([O:8][CH2:9][CH2:10][CH2:11][O:12][C:13]2[CH:28]=[CH:27][C:16]3[CH2:17][CH2:18][CH:19]([CH2:21][CH2:22][C:23]([O:25]C)=[O:24])[O:20][C:15]=3[C:14]=2[CH2:29][CH2:30][CH3:31])=[C:6]([CH2:34][CH:35]2[CH2:37][CH2:36]2)[C:5]=1[O:38][CH3:39])=[O:3]>C(OCC)(=O)C.CO.C(O)(=O)C>[NH2:1][C:2]([C:4]1[CH:33]=[CH:32][C:7]([O:8][CH2:9][CH2:10][CH2:11][O:12][C:13]2[CH:28]=[CH:27][C:16]3[CH2:17][CH2:18][CH:19]([CH2:21][CH2:22][C:23]([OH:25])=[O:24])[O:20][C:15]=3[C:14]=2[CH2:29][CH2:30][CH3:31])=[C:6]([CH2:34][CH:35]2[CH2:37][CH2:36]2)[C:5]=1[O:38][CH3:39])=[O:3]

참가 물질

3

반응물 1

HCID 22399584HCID 22399584, 화합물

생성물 1

HCID 21479718HCID 21479718, 화합물

시약·촉매·용매 1

HCID 22023684HCID 22023684, 화합물용매

실험 절차

The compound of Example 74 is saponified as described in Example 62. Chromatography on silica gel with ethyl acetate/methanol/acetic acid (95:4.5:0.5) as eluant gives the product.

출처 및 근거

ORD 기록
ord-8a34c3849be4453ba4e6ffb402aef1cd
출처 데이터셋
uspto-grants-1992_06
특허 번호
US05124350

반응 노트

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