4-Methylbenzenethiol → p-Toluenesulfenyl chloride

HRID 894261노트

반응식

HRID 894261 반응식
[C:1]1([CH3:8])[CH:6]=[CH:5][C:4]([SH:7])=[CH:3][CH:2]=1.[Cl:9]N1C(=O)CCC1=O>C1C=CC=CC=1>[C:1]1([CH3:8])[CH:6]=[CH:5][C:4]([S:7][Cl:9])=[CH:3][CH:2]=1

참가 물질

4

반응물 2

HCID 78114-MethylbenzenethiolHCID 31398Chlorosuccinimide

생성물 1

HCID 11019146p-Toluenesulfenyl chloride수율 88.2%

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

By the method of Preparation 5, 6.2 g. of p-toluenethiol (6.2 g., 50 mmoles) was reacted with N-chlorosuccinimide (6.67 g., 50 mmoles) in 100 ml. of benzene to yield p-toluenesulfenyl chloride (7.0 g.) as an oil.

후처리

  1. customBy the method of Preparation 5, 6.2 g

출처 및 근거

ORD 기록
ord-74d7decd008644929a1e533342bb9a0a
출처 데이터셋
uspto-grants-1981_08
특허 번호
US04282246

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