Oxalate → HCID 20575151, 화합물

반응식

C([O-])(=O)C([O-])=O.[CH3:7][C:8]1[S:9][C:10]([CH3:20])=[CH:11][C:12]=1[C:13]([C:15]1[CH:19]=[CH:18][S:17][CH:16]=1)=O.Cl[CH:22]1[CH2:27][CH2:26][N:25]([CH3:28])[CH2:24][CH2:23]1.[Mg]>>[S:17]1[CH:18]=[CH:19][C:15]([C:13]([C:12]2[CH:11]=[C:10]([CH3:20])[S:9][C:8]=2[CH3:7])=[C:22]2[CH2:27][CH2:26][N:25]([CH3:28])[CH2:24][CH2:23]2)=[CH:16]1

참가 물질

반응물 4

HCID 71081Oxalate

HCID 793424-chloro-N-methylpiperidine

HCID 5462224Magnesium

HCID 20575148HCID 20575148, 화합물

생성물 1

HCID 20575151HCID 20575151, 화합물

실험 절차

The starting carbinol was obtained in a manner analogous to Example 1 (a), from 12.2 grams (0.055) mole) of (2,5-dimethyl-3-thienyl)-3-thienyl ketone, 14.7 grams (0.11 mole) of 4-chloro-N-methyl-piperidine and 2.67 grams (0.11 gram atom, of magnesium.

출처 및 근거

ORD 기록: ord-1f5806daddff454da3f0c265e59d2240
출처 데이터셋: uspto-grants-1981_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04283405

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