Allyl Isothiocyanate → 3-(4-Bromophenyl)-5-isothiocyanatomethyl-2-isoxazoline

HRID 894322노트

반응식

HRID 894322 반응식
[Br:1][C:2]1[CH:10]=[CH:9][C:5]([CH:6]=[N:7][OH:8])=[CH:4][CH:3]=1.[CH2:11]([N:14]=[C:15]=[S:16])[CH:12]=[CH2:13]>>[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]2[CH2:13][CH:12]([CH2:11][N:14]=[C:15]=[S:16])[O:8][N:7]=2)=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 5971Allyl IsothiocyanateHCID 6080884-Bromobenzaldehyde Oxime

생성물 1

HCID 128896523-(4-Bromophenyl)-5-isothiocyanatomethyl-2-isoxazoline

실험 절차

A 10 g. portion of 4-bromobenzaldoxime was chlorinated and reacted with 10 g. of allylisothiocyanate to prepare 15 g. of product, m.p. 123°-125°.

후처리

  1. customreacted with 10 g

출처 및 근거

ORD 기록
ord-395a8587d90f41a7a679905ab23922ba
출처 데이터셋
uspto-grants-1981_08
특허 번호
US04283403

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