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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 894480생성일: 2026년 10월 24일

Bis(4-hydroxyphenyl)methane → Bis(p-(3-butoxy-2-hydroxypropyloxy)phenyl)methane

https://huagongshe.com/ko/reaction/894480

반응식

참여 물질

역할이름HCID투입량
반응물Bis(4-hydroxyphenyl)methaneHCID 12111—
반응물Butyl glycidyl etherHCID 17049—
촉매Benzyltrimethylammonium chlorideHCID 5963—
생성물Bis(p-(3-butoxy-2-hydroxypropyloxy)phenyl)methaneHCID 20574263—

반응 조건

온도100 °C

반응 단계

Bis(p-hydroxyphenyl)methane (303 g; 1.5 moles), butyl glycidyl ether of epoxide content 7.45 equiv./kg (402.7 g; 6 equiv.), and benzyltrimethylammonium chloride (3 g) were stirred together and heated to 100° C., at which temperature an exothermic reaction commenced. The mixture was kept at 120° C. by moderate cooling and then, when the temperature of the mixture began to fall, heating was resumed, keeping the temperature at 120° C. for 1 hour and 150° C. for 4 hours. The mixture was cooled, and its epoxide content was found to be 0.1 equiv./kg, indicating that the reaction was virtually complete.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04284574
출처 데이터셋uspto-grants-1981_08
ORD IDord-7ca643d425bc45448341e50a01dee08e
출처 메모uspto-grants-1981_08