참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Bisphenol S | HCID 6626 | — |
| 반응물 | Butyl glycidyl ether | HCID 17049 | — |
| 촉매 | Benzyltrimethylammonium chloride | HCID 5963 | — |
| 생성물 | Bis(p-(3-butoxy-2-hydroxypropyloxy)phenyl)sulphone | HCID 19873557 | — |
반응 단계
4,4'-Dihydroxydiphenyl sulphone (125.0 g; 0.5 mole), butyl glycidyl ether of epoxide content 7.45 equiv./kg (134.2 g; 1 equiv.), and benzyltrimethylammonium chloride (1.0 g) were stirred together and heated at 100° C. for 1 hour, at 120° C. for 2 hours, and then at 130° C. for 4 hours. The mixture was cooled, and was found to have an epoxide content of 0.03 equiv./kg, indicating that the reaction was substantially complete.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04284574 |
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| 출처 데이터셋 | uspto-grants-1981_08 |
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| ORD ID | ord-c36a8b87b0d540ffb1f00a301a0c2f60 |
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| 출처 메모 | uspto-grants-1981_08 |
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