Cyclohexene → 6-Methoxy-2-morpholin-4-ylpyrid-3-ylamine

HRID 895304노트

반응식

HRID 895304 반응식
[CH3:1][O:2][C:3]1[N:8]=[C:7]([N:9]2[CH2:14][CH2:13][O:12][CH2:11][CH2:10]2)[C:6]([N+:15]([O-])=O)=[CH:5][CH:4]=1.C1CCCCC=1>[Pd].C(O)C>[CH3:1][O:2][C:3]1[N:8]=[C:7]([N:9]2[CH2:10][CH2:11][O:12][CH2:13][CH2:14]2)[C:6]([NH2:15])=[CH:5][CH:4]=1

참가 물질

5

반응물 2

HCID 8079CyclohexeneHCID 28264174-(6-Methoxy-3-nitropyrid-2-yl)morpholine

생성물 1

HCID 120934016-Methoxy-2-morpholin-4-ylpyrid-3-ylamine

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

6.19 g (0.026 mol) of the product 4-(6-methoxy-3-nitropyrid-2-yl)morpholine synthesized according to the above procedure, 50 ml of ethanol, 20 ml of cyclohexene and 2 g of palladium-on-charcoal were placed in a fully equipped round-bottomed flask.

출처 및 근거

ORD 기록
ord-92bfd378b5734e0d89f5e61d774fbdaa
출처 데이터셋
uspto-grants-2005_07
특허 번호
US06916345B2

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