Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Bromooctane → 5,8,11,14-Tetraoxadocosane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Bromooctane | HCID 8140 | — |
| 반응물 | Diethylene Glycol Monobutyl Ether | HCID 8177 | — |
| 반응물 | Triethylene glycol monobutyl ether | HCID 8923 | — |
| 생성물 | 5,8,11,14-Tetraoxadocosane | HCID 57469342 | — |
반응 단계
The procedure followed that of Reference Example 4, except for use of n-octyl bromide and triethylene glycol n-butyl ether instead of butyl bromide and diethylene glycol butyl ether, respectively. Triethylene glycol n-butyl n-octyl ether (abbreviated as “TEG-BO” hereafter) was obtained by distillation (b.p.: 140-145° C. at 70 Pa). TEG-BO has a corresponding boiling point of about 350° C. under normal pressure. The solubility of glycolide in this compound at 25° C. was 2.0%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06916939B2 |
| 출처 데이터셋 | uspto-grants-2005_07 |
| ORD ID | ord-47778540c5b149ea972ef2ad70b8a597 |
| 출처 메모 | uspto-grants-2005_07 |