Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → Methanaminium, N-methyl-N-(phenylmethylene)-, chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 생성물 | Methanaminium, N-methyl-N-(phenylmethylene)-, chloride | HCID 11073839 | — |
반응 단계
The reaction of 32.0 ml (0.213 mol) dimethylamine solution and 8.0 ml (0.079 mol) benzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 4.7 ml (0.079 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 9.5 g (corresponding to 70.7% of the yield calculated by theory) of benzylidene-dimethyl-ammonium chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07091220B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-a8a93c2e2b784f2fbed88552562dcb80 |
| 출처 메모 | uspto-grants-2006_08 |