Ethyl indole-2-carboxylate → 3-(Dimethylaminophenylmethyl)-1H-indole-2-carboxylic Acid Ethyl Ester

HRID 8981

반응식

HRID 8981 반응식
[CH2:1]([O:3][C:4]([C:6]1[NH:7][C:8]2[C:13]([CH:14]=1)=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:5])[CH3:2].[Cl-].[CH:16](=[N+:23]([CH3:25])[CH3:24])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH2:1]([O:3][C:4]([C:6]1[NH:7][C:8]2[C:13]([C:14]=1[CH:16]([N:23]([CH3:25])[CH3:24])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:5])[CH3:2]

참가 물질

3

반응물 2

HCID 73125Ethyl indole-2-carboxylateHCID 11073839Methanaminium, N-methyl-N-(phenylmethylene)-, chloride

생성물 1

HCID 98802053-(Dimethylaminophenylmethyl)-1H-indole-2-carboxylic Acid Ethyl Ester

실험 절차

The preparation was carried out in accordance with general synthesis instructions 4 from 1H-indole-2-carboxylic acid ethyl ester and benzylidene-dimethyl-ammonium chloride. For characterization, an ESI-MS was recorded:

출처 및 근거

ORD 기록
ord-72da6cfad289430d96716ceae4346d94
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07091220B2

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