1H-indol-4-ol → 3-(Dimethylaminophenylmethyl)-1H-indol-4-ol

반응식

[OH:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][NH:6]2.[Cl-].[CH:12](=[N+:19]([CH3:21])[CH3:20])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH3:20][N:19]([CH:12]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:4]1[C:3]2[C:2]([OH:1])=[CH:10][CH:9]=[CH:8][C:7]=2[NH:6][CH:5]=1)[CH3:21]

참가 물질

반응물 2

HCID 754211H-indol-4-ol

HCID 11073839Methanaminium, N-methyl-N-(phenylmethylene)-, chloride

생성물 1

HCID 98784763-(Dimethylaminophenylmethyl)-1H-indol-4-ol

실험 절차

The preparation was carried out in accordance with general synthesis instructions 4 from 4-hydroxy-1H-indole and benzylidene-dimethyl-ammonium chloride, which had been prepared in accordance with example 1.

후처리

customhad been prepared in accordance with example 1

출처 및 근거

ORD 기록: ord-0be84a70ba3545d5b8875c78bac9b1ac
출처 데이터셋: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07091220B2

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