Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetic acid → (4-{2-[2-(Methoxycarbonyl)phenoxy]ethyl}phenoxy)acetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetic acid | HCID 6422 | — |
| 반응물 | Methyl 2-{2-[4-(2-tert-butoxy-2-oxoethoxy)phenyl]ethoxy}benzoate | HCID 69259306 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | (4-{2-[2-(Methoxycarbonyl)phenoxy]ethyl}phenoxy)acetic acid | HCID 69258392 | 95% |
반응 단계
Methyl 2-{2-[4-(2-tert-butoxy-2-oxoethoxy)phenyl]ethoxy}benzoate (0.400 g, 1.0351 mmol) was dissolved in DCM and trifluoracetic acid (0.8 ml, 8.281 mmol) was added. The mixture was stirred at room temperature for 3 h. The solvent was evaporated to give 325 mg of a white powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07351858B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-03c3e0039056428a82fe06c4ce0e4358 |
| 출처 메모 | uspto-grants-2008_04 |