2'-Nitro[1,1'-biphenyl]-4-ol → HCID 11348665, 화합물

HRID 899529

반응식

HRID 899529 반응식
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=2[N+:14]([O-:16])=[O:15])=[CH:4][CH:3]=1.C[O:18][C:19]([C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([CH2:27]Br)[N:22]=1)=[O:20]>>[N+:14]([C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=1[C:5]1[CH:6]=[CH:7][C:2]([O:1][CH2:27][C:23]2[N:22]=[C:21]([C:19]([OH:20])=[O:18])[CH:26]=[CH:25][CH:24]=2)=[CH:3][CH:4]=1)([O-:16])=[O:15]

참가 물질

3

반응물 2

HCID 155411122'-Nitro[1,1'-biphenyl]-4-olHCID 21471714Methyl 6-(bromomethyl)pyridine-2-carboxylate2회

생성물 1

HCID 11348665HCID 11348665, 화합물

실험 절차

6-(2′-Nitro-biphenyl-4-yloxymethyl)-pyridine-2-carboxylic acid was prepared using general procedure B from from 4-hydroxy-2′-nitrobiphenyl (available from TCI America, Portland, Oreg.) and 6-bromomethyl-pyridine-2-carboxylic acid methyl ester (Intermediate 2). Yield: 62 mg. Mass spectrum (ES) MH+=351.

출처 및 근거

ORD 기록
ord-120fd1249bf84bc1b720d104a5507404
출처 데이터셋
uspto-grants-2008_04
특허 번호
US07355049B2

연결된 노트

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