Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrofuran → 3-Octanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | 2-Ethylhexanal | HCID 31241 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 생성물 | 3-Octanol | HCID 11527 | 99.5% |
반응 단계
3 g of catalyst A (3% Ru/SiO2) were placed in a 300 ml pressure reactor. The reactor was subsequently charged with 150 ml of a 33% strength solution of 2-ethylhexanal in THF. The hydrogenation was carried out at 130° C. and a pressure of 250 bar using pure hydrogen. The hydrogenation was continued until no more hydrogen was taken up and the reactor was subsequently vented. After distilling off the solvent, the reaction product was analyzed by gas chromatography. 2-Ethylhexanal had been reacted completely. 99.5% of ethylhexanol were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07355084B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-2456a73224064c9594f284f23b30ea77 |
| 출처 메모 | uspto-grants-2008_04 |