Methacrylic Acid → 1-Ethoxyethyl Methacrylate (stabilized with MEHQ)
반응식
[C:1]([OH:6])(=[O:5])[C:2]([CH3:4])=[CH2:3].[CH:7]([O:9][CH2:10][CH3:11])=[CH2:8].O.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[C:1]([O:6][CH:7]([O:9][CH2:10][CH3:11])[CH3:8])(=[O:5])[C:2]([CH3:4])=[CH2:3]참가 물질
4
실험 절차
To a mixture of 1.00 g of methacrylic acid and 0.836 g of ethyl vinyl ether was added 2 mg of p-toluenesulfonic acid monohydrate, and a reaction was allowed at room temperature for 1 hour. The conversion ratio of methacrylic acid was 82%, with the conversion ratio of ethyl vinyl ether of 94%. Accordingly, 1-ethoxyethyl methacrylate was obtained with the reaction yield of 80% and the selection ratio to ethyl vinyl ether of 85%, and a polymer of ethyl vinyl ether was produced.
출처 및 근거
- ORD 기록
- ord-069a77f2b55e4a538d01927f9f4c4b4b
- 출처 데이터셋
- uspto-grants-2008_04
- 특허 번호
- US07358030B2
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