6-Ethoxypyridin-3-amine → (6-Ethoxy-pyridin-3-yl)-isopropyl-amine

HRID 900122

반응식

HRID 900122 반응식
Cl[C:2]1[N:7]=[CH:6][C:5]([NH:8][CH:9]([CH3:11])[CH3:10])=[CH:4][CH:3]=1.[CH2:12]([O:14]C1N=CC(N)=CC=1)[CH3:13]>CC(C)=O>[CH2:12]([O:14][C:2]1[N:7]=[CH:6][C:5]([NH:8][CH:9]([CH3:11])[CH3:10])=[CH:4][CH:3]=1)[CH3:13]

참가 물질

4

반응물 2

HCID 30403016-Ethoxypyridin-3-amineHCID 589579206-chloro-N-(propan-2-yl)pyridin-3-amine

생성물 1

HCID 58957938(6-Ethoxy-pyridin-3-yl)-isopropyl-amine

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

Following the procedure described for Preparation 2(A), 6-ethoxy-pyridin-3-ylamine (10 g, 72.4 mmol) was reacted with acetone (4.8 mL) to provide 11.18 g of (6-ethoxy-pyridin-3-yl)-isopropyl-amine. 1H NMR (CD3OD) δ 7.48 (d, 1H), 7.11 (dd, 1H), 6.61 (d, 1H), 4.14 (q, 2H), 3.48 (m, 1H), 1.32 (t, 3H), 1.14 (d, 6H); MS 181.3 (M+1).

출처 및 근거

ORD 기록
ord-962deba8319d4c39a96ddbc4e6364ddd
출처 데이터셋
uspto-grants-2008_04
특허 번호
US07358242B2

연결된 노트

불러오는 중…