참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | Methyl cyclohexanecarboxylate | HCID 20748 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Cyclohexanecarbohydrazide | HCID 240039 | 33.5% |
반응 단계
To a solution of methyl cyclohexane carboxylate (12 g, 83.9 mmol) in MeOH (50 mL) was added hydrazine (5.3 mL, 1.67 mol). The reaction mixture was heated at 65° C. overnight. The reaction mixture was cooled to room temperature and the resultant solid was collected by filtration and was dried in vacuo to give 4.0 g of cyclohexanecarboxylic acid hydrazide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07358242B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_04 |
|---|
| ORD ID | ord-0f7b1b1ab58e47aa88a8b07dc365b917 |
|---|
| 출처 메모 | uspto-grants-2008_04 |
|---|
