Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → N-(3-cyanothiophen-2-yl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 2-Aminothiophene-3-carbonitrile | HCID 736607 | — |
| 생성물 | N-(3-cyanothiophen-2-yl)acetamide | HCID 676450 | — |
반응 단계
2-Amino-3-cyanothiophene (12 g) was heated at reflux in acetic anhydride (34 ml) for 15 minutes, cooled and refrigerated for 3 h. The crystalline product was filtered off (13.6 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07358376B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-253eee24c3de45a79cbb8584166f4291 |
| 출처 메모 | uspto-grants-2008_04 |