Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromine → 2-Bromophenacyl Bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 2'-Bromoacetophenone | HCID 75060 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 2-Bromophenacyl Bromide | HCID 2737522 | — |
반응 단계
Bromine (40.3 g, 0.25 mol) was added dropwise to a solution of 2′-Bromoacetophenone (50.0 g, 0.25 mol) in acetic acid (500 ml) over 1.5 hours at 15-20° C. The solution was then allowed to warm to room temperature and concentrated under reduced pressure to yield a crude product that was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07361656B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-bfd65b15d78b4f88a52cb876e178cb05 |
| 출처 메모 | uspto-grants-2008_04 |