Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → (2-Methyl-benzylidene)-dimethylammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | 2-Methylbenzaldehyde | HCID 10722 | — |
| 생성물 | (2-Methyl-benzylidene)-dimethylammonium chloride | HCID 21985341 | — |
반응 단계
The reaction of 14.0 ml (0.108 mol) dimethylamine solution and 4.6 ml (0.040 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 2.4 ml (0.040 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.3 g (corresponding to 73% of the yield calculated by theory) dimethyl-(2-methyl-benzylidene)-ammonium chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07091220B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-9d6a01b849784a7f99927f8025b4abe7 |
| 출처 메모 | uspto-grants-2006_08 |