Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Isopropylaniline → HCID 178439243, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Isopropylaniline | HCID 7464 | — |
| 반응물 | 4-(Methylsulfonyl)benzonitrile | HCID 519981 | — |
| 생성물 | HCID 178439243 | HCID 178439243 | 60% |
반응 단계
The title compound was prepared from 4-methylsulfonylbenzonitrile (5.43 g, 30 mmol) and 4-isopropylaniline (4.05 g, 30 mmol) by following the procedure described in preparation 1 (5.66 g, yield 60%, purity 88% by HPLC). 1H-NMR (CDCl3):δ 1.25-1.27 (d, 6H), 2.9-2.95 (m, 1H), 3.07 (s, 3H), 4.92 (bs, 2H, D2O exchangeable), 6.90-6.92 (d, 2H), 7.23-7.26 (d, 2H), 8.01-8.03 (d, 2H), 8.08-8.1 (d, 2H). MS m/z:317.2 (M+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07365069B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-0bfd268215da41f79ebf9c3bf0464de5 |
| 출처 메모 | uspto-grants-2008_04 |