Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4-Dimethylaniline → HCID 178426511, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4-Dimethylaniline | HCID 7248 | — |
| 반응물 | 4-(Methylsulfonyl)benzonitrile | HCID 519981 | — |
| 생성물 | HCID 178426511 | HCID 178426511 | 45% |
반응 단계
The title compound was prepared from 4-methylsulfonylbenzonitrile (5.0 g, 28 mmol) and 3,4-dimethylaniline (3.36 g, 28 mmol) by following the procedure described in preparation 1 (3.75 g, yield 45%, purity 97.1% by HPLC). 1H-NMR (CDCl3):δ 2.25-2.26 (d, 6H), 3.07 (s, 3H), 4.91 (bs, 2H, D2O exchangeable), 6.71-6.73 (m, 1H), 6.78 (s, 1H), 7.12-7.14 (d, 1H), 8-8.02 (d, 2H), 8.07-8.09 (d, 2H). MS m/z:303.2 (M+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07365069B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-f7ce2b67b72a4bc3868e4d22563141db |
| 출처 메모 | uspto-grants-2008_04 |