Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → 2-Methoxy-benzylidene-dimethyl-ammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | 2-Methoxybenzaldehyde | HCID 8658 | — |
| 생성물 | 2-Methoxy-benzylidene-dimethyl-ammonium chloride | HCID 21985303 | — |
반응 단계
The reaction of 17.0 ml (0.135 mol) dimethylamine solution and 6.8 g ml (0.050 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 3.0 ml (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 4.8 g (corresponding to 48% of the yield calculated by theory) 2-methoxy-benzylidene-dimethyl-ammonium chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07091220B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-6fc688613ae646f2a32ab26807d5074f |
| 출처 메모 | uspto-grants-2006_08 |