5-Amino-3-methyl-1-(4-chloro-2-methylphenyl) pyrazole → 1-Acetyl-2[1(4-chloro-2-methylphenyl)-3-methyl-5-pyrazolyl] amino-2-imidazoline

HRID 903074

반응식

HRID 903074 반응식
[NH2:1][C:2]1[N:6]([C:7]2[CH:12]=[CH:11][C:10]([Cl:13])=[CH:9][C:8]=2[CH3:14])[N:5]=[C:4]([CH3:15])[CH:3]=1.[C:16]([N:19]1[CH2:23][C:22](=O)[N:21]=[CH:20]1)(=[O:18])[CH3:17]>>[C:16]([N:19]1[CH2:23][CH2:22][N:21]=[C:20]1[NH:1][C:2]1[N:6]([C:7]2[CH:12]=[CH:11][C:10]([Cl:13])=[CH:9][C:8]=2[CH3:14])[N:5]=[C:4]([CH3:15])[CH:3]=1)(=[O:18])[CH3:17]

참가 물질

3

반응물 2

HCID 127637865-Amino-3-methyl-1-(4-chloro-2-methylphenyl) pyrazoleHCID 22350258N-acetyl-2-imidazolinone

생성물 1

HCID 127638021-Acetyl-2[1(4-chloro-2-methylphenyl)-3-methyl-5-pyrazolyl] amino-2-imidazoline

실험 절차

5-Amino-3-methyl-1-(4-chloro-2-methylphenyl) pyrazole (22.16 g.) and 1-acetyl-2-imidazolinone (15.4 g.) were reacted as described in Example I to give 13.1 g. of product, mp 195°-195°.

후처리

  1. customto give 13.1 g

출처 및 근거

ORD 기록
ord-2c8a9a4cf8bb48c09cc59a34e2d4163e
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04226773

연결된 노트

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