Diphenyllead dichloride → Diphenyl lead salicylaldehyde

HRID 903105노트

반응식

HRID 903105 반응식
[C:1]1([Pb:7](Cl)(Cl)[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:16](=[O:24])[C:17]1[C:18](=[CH:20][CH:21]=[CH:22][CH:23]=1)[OH:19].[Na]>CC(C)=O>[CH:16](=[O:24])[C:17]1[C:18](=[CH:20][CH:21]=[CH:22][CH:23]=1)[OH:19].[C:8]1([Pb:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1

참가 물질

4

반응물 2

HCID 75032Diphenyllead dichlorideHCID 86741752Sodium 2-formylbenzenolate

생성물 1

HCID 88776750Diphenyl lead salicylaldehyde

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

Diphenyl lead dichloride (0.01 mol) is mixed with 0.02 mol of sodium salicylaldehyde in acetone. The solution is allowed to stand 10 minutes and then filtered. Water is added to the filtrate to precipitate the lead chelate complex, which is then separated by filtration.

후처리

  1. filtrationfiltered
  2. additionWater is added to the filtrate
  3. customto precipitate the lead chelate complex, which
  4. customis then separated by filtration

출처 및 근거

ORD 기록
ord-6ffbe9600a994d89abad6953696604cd
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04226792

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