Imidazole → HCID 23337927, 화합물

HRID 903164노트

반응식

HRID 903164 반응식
[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.Br[C:7]1[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][C:15]#[N:16])=[CH:9][CH:8]=1.C(=O)([O-])[O-].[K+].[K+]>[N+](C1C=CC=CC=1)([O-])=O>[N:1]1([C:7]2[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][C:15]#[N:16])=[CH:9][CH:8]=2)[CH:5]=[CH:4][N:3]=[CH:2]1

참가 물질

5

반응물 3

HCID 795ImidazoleHCID 11430Potassium CarbonateHCID 27356113-(4-Bromophenyl)propanenitrile

생성물 1

HCID 23337927HCID 23337927, 화합물

시약·촉매·용매 1

HCID 7416Nitrobenzene용매

반응 조건

온도
160 °C

실험 절차

A mixture of 2.8 g of imidazole, 7.6 g of 3-(p-bromophenyl)propionitrile, 4.7 g of anhydrous potassium carbonate, and 0.4 g of cuprous bromide in 15 ml of nitrobenzene was heated at 160° C. for 25 hours under stirring.

출처 및 근거

ORD 기록
ord-21b1c048480943a9b2344229bc5f6544
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04226878

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