Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylamine → N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylamine | HCID 8021 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | p-Menthane-3-carboxylic acid | HCID 97896 | — |
| 반응물 | Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)- | HCID 13734319 | — |
| 생성물 | N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide | HCID 93591 | — |
반응 단계
Following the procedure of Example 5, p-menthane-3-carboxylic acid (1.84 g.) was reacted with thionyl chloride and the p-menth-3-oyl chloride then reacted with diethylamine (0.74 g.) in the presence of sodium hydroxide (0.4 g.). The product N,N-diethyl-p-menthane-3-carboxamide was recovered.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04226988 |
| 출처 데이터셋 | uspto-grants-1980_10 |
| ORD ID | ord-55af27376aad4328a0e398514800ad87 |
| 출처 메모 | uspto-grants-1980_10 |